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The Resource Interpretation of organic spectra, by Yong-Cheng Ning

Interpretation of organic spectra, by Yong-Cheng Ning

Label
Interpretation of organic spectra
Title
Interpretation of organic spectra
Statement of responsibility
by Yong-Cheng Ning
Creator
Subject
Language
eng
Cataloging source
DLC
http://library.link/vocab/creatorName
Ning, Yong-Cheng
Illustrations
illustrations
Index
index present
Literary form
non fiction
Nature of contents
bibliography
http://library.link/vocab/subjectName
  • Spectrum analysis
  • Organic compounds
Label
Interpretation of organic spectra, by Yong-Cheng Ning
Instantiates
Publication
Bibliography note
Includes bibliographical references and index
Contents
  • Factors affecting chemical shifts
  • 3.4.
  • Long-range heteronuclear shift correlation spectroscopy
  • 3.5.
  • NOESY and ROESY
  • 3.6.
  • Total correlation spectroscopy, TOCSY
  • References
  • 4.
  • Interpretation of mass spectra
  • 4.1.
  • 1.2.
  • Basic knowledge of organic mass spectrometry
  • 4.1.1.
  • Mass spectra
  • 4.1.2.
  • Ionization in organic mass spectrometry
  • 4.1.3.
  • Ion types in organic mass spectrometry
  • 4.2.
  • Isotopic ion clusters in mass spectra
  • 4.3.
  • Coupling constant J
  • Interpretation of EI MS
  • 4.3.1.
  • Determination of molecular ion peak
  • 4.3.2.
  • Interpretation of fragment ion peaks
  • 4.3.3.
  • Interpretation of rearrangement ion peaks
  • 4.3.4.
  • Complex cleavages of alicyclic compounds
  • 4.3.5.
  • 1.2.1.
  • Mass spectrum patterns of common functional groups
  • 4.3.6.
  • Interpretation of the EI mass spectrum and examples
  • 4.4.
  • Interpretation of the mass spectra from soft ionization
  • 4.4.1.
  • Mass spectra from ESI (electrospray ionization)
  • 4.4.2.
  • Mass spectra from CI
  • 4.4.3.
  • Coupling effect and coupling constant J
  • Mass spectra from FAB
  • 4.4.4.
  • Mass spectra from MALDI
  • 4.4.5.
  • Mass spectra from APCI
  • 4.4.6.
  • Examples of the interpretation of mass spectra from soft ionization
  • 4.5.
  • Interpretation of high resolution mass spectra
  • 4.6.
  • 1.2.2.
  • Interpretation of mass spectra from tandem mass spectrometry
  • References
  • 5.
  • Interpretation of infrared spectra
  • 5.1.
  • Elementary knowledge of infrared spectroscopy
  • 5.1.1.
  • Infrared spectrum
  • 5.1.2.
  • Two regions of the infrared spectrum
  • Discussion of coupling constants according to their kinds
  • 5.2.
  • Characteristic absorption frequencies of functional groups
  • 5.2.1.
  • Elemental equation of IR spectroscopy
  • 5.2.2.
  • Factors affecting absorption frequencies
  • 5.2.3.
  • Characteristic frequencies of common functional groups
  • 5.3.
  • Discussion on the IR spectrum according to regions
  • 1.3.
  • 5.3.1.
  • Functional group region
  • 5.3.2.
  • Fingerprint region
  • 5.4.
  • Interpretation of IR spectra according to regions
  • 5.5.
  • Interpretation of IR spectra
  • 5.5.1.
  • Key points for the interpretation of IR spectra
  • Chemical equivalence and magnetic equivalence
  • 5.5.2.
  • Steps for the interpretation of an IR spectrum
  • 5.5.3.
  • Searching standard IR spectra from IR spectrum collections or websites
  • 5.5.4.
  • Examples of interpreting IR spectra
  • 6.
  • Identification of unknown compounds or confirmation of structures through comprehensive interpretation of spectra
  • 6.1.
  • Commonly used method and steps
  • 1.3.1.
  • 6.1.1.
  • 1H spectrum
  • 6.1.2.
  • 13C spectrum
  • 6.1.3.
  • DEPT spectrum
  • 6.1.4.
  • COSY spectrum
  • 6.1.5.
  • HMQC (or HSQC) spectrum
  • Machine generated contents note:
  • Chemical equivalence
  • 6.1.6.
  • HMBC spectrum
  • 6.2.
  • Examples for the deduction of the structure of an unknown compound or for the confirmation of an anticipated structure
  • Reference
  • 1.3.2.
  • Magnetic equivalence
  • 1.3.3.
  • Classification of 1H spectra
  • 1.4.
  • Characteristics of the 1H spectra of some functional groups
  • 1.4.1.
  • Substituted phenyl ring
  • 1.4.2.
  • 1.
  • Substituted heteroaromatic ring
  • 1.4.3.
  • Normal long-chain alkyl group
  • 1.4.4.
  • Carbonyl compounds
  • 1.4.5.
  • Reactive hydrogen atom
  • 1.4.6.
  • Compounds containing fluorine or phosphor atoms
  • 1.5.
  • Interpretation of 1H NMR spectra
  • Interpretation of 1H NMR spectra
  • 1.5.1.
  • Find impurity peaks, pay attention to the solvent applied
  • 1.5.2.
  • Calculation of the unsaturation number of the unknown compound
  • 1.5.3.
  • Determination of the number of hydrogen atoms corresponding to every peak set in the 1H spectrum
  • 1.5.4.
  • Determination of functional groups of the unknown compound
  • 1.5.5.
  • 1.1.
  • Analysis of coupling splittings of peak sets
  • 1.5.6.
  • Combination of possible structural units
  • 1.5.7.
  • Assignment of the 1H spectrum according to the deduced structure
  • 1.5.8.
  • Checking of the deduced structure
  • 1.6.
  • Examples of 1H spectrum interpretation
  • Reference
  • Chemical shift
  • 2.
  • Interpretation of 13C NMR spectra
  • 2.1.
  • Characteristics and advantages of the 13C NMR spectra
  • 2.2.
  • The main parameter of the 13C spectrum is the chemical shift
  • 2.3.
  • Chemical shift values of common functional groups and main factors affecting chemical shift values
  • 2.3.1.
  • Alkanes and their derivatives
  • 1.1.1.
  • 2.3.2.
  • Cycloalkanes and their derivatives
  • 2.3.3.
  • Alkylenes and their derivatives
  • 2.3.4.
  • Benzene and its derivatives
  • 2.3.5.
  • Carbonyl groups
  • 2.4.
  • Determination of the carbon atom orders
  • Conception of chemical shift
  • 2.5.
  • Steps for 13C NMR spectrum interpretation
  • 2.5.1.
  • Recognizing impurity peaks and identifying solvent peaks
  • 2.5.2.
  • Calculation of the unsaturation number of the unknown compound
  • 2.5.3.
  • Consideration of chemical shift values of peaks
  • 2.5.4.
  • Determination of carbon atom orders
  • 1.1.2.
  • 2.5.5.
  • Postulation of possible functional groups
  • 3.
  • Interpretation of 2D NMR spectra
  • 3.1.
  • General knowledge about 2D NMR spectra
  • 3.2.
  • Homonuclear shift correlation spectroscopy, COSY (H, H-COSY)
  • 3.3.
  • Heteronuclear shift correlation spectroscopy
Control code
ocn669751079
Dimensions
26 cm
Extent
xii, 412 p.
Isbn
9780470825167
Isbn Type
(hardback)
Lccn
2010051188
Other physical details
ill.
System control number
(OCoLC)669751079
Label
Interpretation of organic spectra, by Yong-Cheng Ning
Publication
Bibliography note
Includes bibliographical references and index
Contents
  • Factors affecting chemical shifts
  • 3.4.
  • Long-range heteronuclear shift correlation spectroscopy
  • 3.5.
  • NOESY and ROESY
  • 3.6.
  • Total correlation spectroscopy, TOCSY
  • References
  • 4.
  • Interpretation of mass spectra
  • 4.1.
  • 1.2.
  • Basic knowledge of organic mass spectrometry
  • 4.1.1.
  • Mass spectra
  • 4.1.2.
  • Ionization in organic mass spectrometry
  • 4.1.3.
  • Ion types in organic mass spectrometry
  • 4.2.
  • Isotopic ion clusters in mass spectra
  • 4.3.
  • Coupling constant J
  • Interpretation of EI MS
  • 4.3.1.
  • Determination of molecular ion peak
  • 4.3.2.
  • Interpretation of fragment ion peaks
  • 4.3.3.
  • Interpretation of rearrangement ion peaks
  • 4.3.4.
  • Complex cleavages of alicyclic compounds
  • 4.3.5.
  • 1.2.1.
  • Mass spectrum patterns of common functional groups
  • 4.3.6.
  • Interpretation of the EI mass spectrum and examples
  • 4.4.
  • Interpretation of the mass spectra from soft ionization
  • 4.4.1.
  • Mass spectra from ESI (electrospray ionization)
  • 4.4.2.
  • Mass spectra from CI
  • 4.4.3.
  • Coupling effect and coupling constant J
  • Mass spectra from FAB
  • 4.4.4.
  • Mass spectra from MALDI
  • 4.4.5.
  • Mass spectra from APCI
  • 4.4.6.
  • Examples of the interpretation of mass spectra from soft ionization
  • 4.5.
  • Interpretation of high resolution mass spectra
  • 4.6.
  • 1.2.2.
  • Interpretation of mass spectra from tandem mass spectrometry
  • References
  • 5.
  • Interpretation of infrared spectra
  • 5.1.
  • Elementary knowledge of infrared spectroscopy
  • 5.1.1.
  • Infrared spectrum
  • 5.1.2.
  • Two regions of the infrared spectrum
  • Discussion of coupling constants according to their kinds
  • 5.2.
  • Characteristic absorption frequencies of functional groups
  • 5.2.1.
  • Elemental equation of IR spectroscopy
  • 5.2.2.
  • Factors affecting absorption frequencies
  • 5.2.3.
  • Characteristic frequencies of common functional groups
  • 5.3.
  • Discussion on the IR spectrum according to regions
  • 1.3.
  • 5.3.1.
  • Functional group region
  • 5.3.2.
  • Fingerprint region
  • 5.4.
  • Interpretation of IR spectra according to regions
  • 5.5.
  • Interpretation of IR spectra
  • 5.5.1.
  • Key points for the interpretation of IR spectra
  • Chemical equivalence and magnetic equivalence
  • 5.5.2.
  • Steps for the interpretation of an IR spectrum
  • 5.5.3.
  • Searching standard IR spectra from IR spectrum collections or websites
  • 5.5.4.
  • Examples of interpreting IR spectra
  • 6.
  • Identification of unknown compounds or confirmation of structures through comprehensive interpretation of spectra
  • 6.1.
  • Commonly used method and steps
  • 1.3.1.
  • 6.1.1.
  • 1H spectrum
  • 6.1.2.
  • 13C spectrum
  • 6.1.3.
  • DEPT spectrum
  • 6.1.4.
  • COSY spectrum
  • 6.1.5.
  • HMQC (or HSQC) spectrum
  • Machine generated contents note:
  • Chemical equivalence
  • 6.1.6.
  • HMBC spectrum
  • 6.2.
  • Examples for the deduction of the structure of an unknown compound or for the confirmation of an anticipated structure
  • Reference
  • 1.3.2.
  • Magnetic equivalence
  • 1.3.3.
  • Classification of 1H spectra
  • 1.4.
  • Characteristics of the 1H spectra of some functional groups
  • 1.4.1.
  • Substituted phenyl ring
  • 1.4.2.
  • 1.
  • Substituted heteroaromatic ring
  • 1.4.3.
  • Normal long-chain alkyl group
  • 1.4.4.
  • Carbonyl compounds
  • 1.4.5.
  • Reactive hydrogen atom
  • 1.4.6.
  • Compounds containing fluorine or phosphor atoms
  • 1.5.
  • Interpretation of 1H NMR spectra
  • Interpretation of 1H NMR spectra
  • 1.5.1.
  • Find impurity peaks, pay attention to the solvent applied
  • 1.5.2.
  • Calculation of the unsaturation number of the unknown compound
  • 1.5.3.
  • Determination of the number of hydrogen atoms corresponding to every peak set in the 1H spectrum
  • 1.5.4.
  • Determination of functional groups of the unknown compound
  • 1.5.5.
  • 1.1.
  • Analysis of coupling splittings of peak sets
  • 1.5.6.
  • Combination of possible structural units
  • 1.5.7.
  • Assignment of the 1H spectrum according to the deduced structure
  • 1.5.8.
  • Checking of the deduced structure
  • 1.6.
  • Examples of 1H spectrum interpretation
  • Reference
  • Chemical shift
  • 2.
  • Interpretation of 13C NMR spectra
  • 2.1.
  • Characteristics and advantages of the 13C NMR spectra
  • 2.2.
  • The main parameter of the 13C spectrum is the chemical shift
  • 2.3.
  • Chemical shift values of common functional groups and main factors affecting chemical shift values
  • 2.3.1.
  • Alkanes and their derivatives
  • 1.1.1.
  • 2.3.2.
  • Cycloalkanes and their derivatives
  • 2.3.3.
  • Alkylenes and their derivatives
  • 2.3.4.
  • Benzene and its derivatives
  • 2.3.5.
  • Carbonyl groups
  • 2.4.
  • Determination of the carbon atom orders
  • Conception of chemical shift
  • 2.5.
  • Steps for 13C NMR spectrum interpretation
  • 2.5.1.
  • Recognizing impurity peaks and identifying solvent peaks
  • 2.5.2.
  • Calculation of the unsaturation number of the unknown compound
  • 2.5.3.
  • Consideration of chemical shift values of peaks
  • 2.5.4.
  • Determination of carbon atom orders
  • 1.1.2.
  • 2.5.5.
  • Postulation of possible functional groups
  • 3.
  • Interpretation of 2D NMR spectra
  • 3.1.
  • General knowledge about 2D NMR spectra
  • 3.2.
  • Homonuclear shift correlation spectroscopy, COSY (H, H-COSY)
  • 3.3.
  • Heteronuclear shift correlation spectroscopy
Control code
ocn669751079
Dimensions
26 cm
Extent
xii, 412 p.
Isbn
9780470825167
Isbn Type
(hardback)
Lccn
2010051188
Other physical details
ill.
System control number
(OCoLC)669751079

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